Thermo scientific icap q software manual pn 1288010, revision b 11 chapter 1 using this manual this icap q software manual introduces the software suite qtegra and describes the configuration and operation of the icap q instrument with qtegra. The get ready feature takes your icap rq icpms from standby to. Pdf inductively coupled plasma mass spectrometry icp ms. What do i do if i start uploading documents and cant complete the upload because the system cannot accommodate them. Minimal installation and bench space requirements ensure any laboratory will benefit from this technology. Inductively coupled plasma mass spectrometry icp ms. Drinking water compliance monitoring using us epa method. A large range of elements can be detected using an icp ms, which are summarized in figure 1 below. The determination of major and trace elements in milk using icpq. Our icpms and icpqqq instruments offer the highest matrix tolerance and unmatched interference removal, delivering fast, accurate and consistently reproducible results even for trace metals. Interface thermo fisher scientific icap q operating manual pn 1288090, revision b 37. Overview to scale the picture below is a simulation at scale of the thermo icap q icp ms mass spectrometer system, installed on a ionbench ms mass spec benchtable.
Manuals picture pn description quantity 1288090 icap q operating manual 1 1288021 icap q preinstallation requirements guide 1 table 11. Multielement analysis of single particles and cells icptof. Antivirus and malware prevention in goanywhere mft. Thermo scientific ics5000 was coupled to the icap q for subsequent speciation determinations. See the respective chapters of the manual for details and additional instrument properties. Easytouse system developed to support ultralow detection limits, and has improved interference removal capabilities. Yag 266 nm laser ablation load coil torch cones inductively coupled plasma interface vacuum pumps quadrupole lens mass spectrometer. Thermo scientific icap q icpms industrial area of thessaloniki, block no. It atomizes the sample and creates atomic and small polyatomic ions, which are then detected. Inductively coupled plasma mass spectrometry icpms with. Apr 26, 2017 7 icp ms it is a multielement analysis technique where the icp source converts the atoms of the elements in the sample to ions. Qtegra software platform, there is no need for additional software.
The bench surface should ideally be 80 to 85 cm above the floor. Ergonomically designed quadrupole icp ms with smallest bench space availableinnovat. Experience a dramatically different icpms for total reliability with maximized uptime and a dramatically simplified workflow with the thermo scienti. Choose the thermo scientific icap rq icpms for a complete. Autodilution higher throughput, lower maintenance and autodilution reduce time and cost. Low cost per sample operator time is freed up with simple workflows and a minimal number of steps per task.
This dual mode technology enables advanced flexibility for optimization, quantification and internal standardization. Each pillar is carefully optimized to deliver simplicity, productivity, efficiency and quality in your laboratory. Elemental scientific specializes in inert and highsensitivity sample introduction systems for icp aes and icp ms elemental analysis. Thermo scientific icap 7000 series icpoes genecraft labs. Our extensive product line contains sample introduction devices for all models of. Tubing for sampler has been changed, torch has been changed, cones and lenses cleaned. Autotuning fails, mass calibration fails, cross calibration fails. Inductively coupled plasma mass spectroscopy icpms. Elemental scientific specializes in inert and highsensitivity sample introduction systems for icpaes and icpms elemental analysis. Mar 02, 2016 your icp works by ionising the elements and passing these elements into the ms. Your icp works by ionising the elements and passing these elements into the ms. Our product line consists of autosamplers, microflow pfa nebulizers, concentric nebulizers, apex desolvation nebulizers, pc3 peltier coolers, mp2 micro peristaltic pumps, fast solutions, application solutions and consumables.
Overall it is a cheaper option if the elements do not need lower detection limit like icpms does. Currently, one of the greatest challenges in water analysis is the monitoring of multiple metals in a large number of samples with varying concentrations. To run a measurement the appropriate experiment configuration has to be loaded. Determination of trace elements in waters and wastes. Simplicity and easeofuse work in concert to streamline workflows and achieve rightfirsttime results. The thermo scientific icap q icpms was validated for use against revision 5. The icap q icp ms has been developed with groundbreaking technology to enable advanced highperformance analysis combined with total reliability and ultraflexibility. Instrument control is used by the manager to switch on, optimize and calibrate the icap q instrument. It describes the modes of operation and principle hardware components of your icap q mass spectrometer and provides stepbystep instructions for cleaning and maintaining your instrument. Ergonomically designed quadrupole icpms with smallest bench space availableinnovat.
Impurities are a prevalent issue in the semiconductor industry, particularly semiconductor wafer production. The vacuum pump edwards is enclosed in the noise reduction cabinet, under your mass spectrometer icap q icpms. The icapq icpms system from thermo scientific youtube. Daily performance check in icpms scientist solutions. View online or download thermo scientific icap rq icpms preinstallation requirements manual. Please answer all of the following and return the completed form to us. Icpmass spectrometry the 30minute guide to icpms a worthy member of the inorganic analysis team for nearly 30 years, inductively coupled plasmamass spectrometry icpms has been gaining favor with laboratories around the world as the instrument of choice for performing trace metal analysis. Agilents marketleading inductively coupled plasma mass spectrometry icpms systems provide flexible and reliable solutions for elemental analysis. The icap tqs icp ms system from thermo scientific offers high performance icp ms for ultratrace quantification of trace elements in a variety of semiconductors. The coupling of the ics5000 ion chromatographic system with the icap q icpms has been shown to be a powerful tool for the detection of low concentrations of. Drinking water compliance monitoring using us epa method 200. In meeting this, agilent has developed a range of advanced applications for its portfolio of highproductivity instruments that deliver the sensitivity needed across a wide dynamic range. As shown in figure 1, icp ms consists of an ion source icp, a sampling interface, ion lens, a mass spectrophotometer and a detector.
Thermo scientific qtegra intelligent scientific data solution. Technical data icap rq 2channel instrument the table summarizes the most important technical data of the icap rq icpms systems. The thermo scientific icap tq icpms is the solution to futureproofing. Elements detectable by icp ms analysis perkinelmer. Elemental imaging and petrovolcanological applications of an. Parameter specification value instrument dimensions icap rq icpms length. An innovative multistage peltiercooled desolvation system combined in series with a helical eptfe fluoropolymer membrane desolvator gives maximum icpms signal while simultaneously reading the lowest ratios of oxide. Inductively coupled plasma mass spectrometry wikipedia. Inductively coupled plasmamass spectrometry icpms is a powerful tool for analyzing trace metals in environmental samples. The reliability, analytical performance and ease of use needed to meet the demands of the. The icap 7000 series icpoes offers three models, all of which enable global regulatory compliance, in a wide range of fields, and each instrument is designed to suit the specific throughput requirements of a variety of users. The thermo scientific qtegra intelligent scientific data solution isds is a software platform built on four pillars. Single quadrupole inductively coupled plasma mass spectrometry sqicpms thermo fisher scientific us.
The icap q gc icp ms coupling kit incorporates a unique dual mode sample introduction system for the simultaneous introduction of a liquid in parallel to the gc outlet. Thermo scientific icp techniques, reduces training requirements and makes the addition of a sqicpms into your lab a simple process. Icap is easy to implement since it leverages apache code. Analysis of pharmaceutical products for their elemental impurities. As shown in figure 1, icpms consists of an ion source icp, a sampling interface, ion lens, a mass spectrophotometer and a detector. Br43207 thermo scientific icap q brochure pragolab. It is known and used for its ability to detect metals and several nonmetals in liquid samples at very low concentrations.
Multielement determination in food samples using the thermo. We have had an icap q icp ms installed for the last couple of months. Instrument control overview thermo scientific icap q software manual pn 1288010, revision b 25. Ionbench with the thermo icap q icpms mass spectrometer.
The esi prepfast 2 autodilution system is fully integrated for seamless. The ms relies on the charge of the ions to separate the masses and assumes that all ions are singly charged. Elemental scientific improve icpms lab results with. Inductively coupled plasma mass spectrometry icpms. Thermo scientific icap q icpms rob henry and julian wills, thermo fisher scientific, germany application note 43127 key words icap q, us epa method 200. The thermo scientific icap tq icpms is the solution to futureproofing your laboratory. The icap q instrument is designed to be placed on a bench with its rear panel against a wall. When a new file is uploaded to goanywhere mft, the file contents can be sent to the antivirus software for scanning. Therefore, no security changes to the existing network are likely. The vacuum pump edwards is enclosed in the noise reduction cabinet, under your mass spectrometer icap q icp ms. The operating condition of the icpms and the specifications of each configuration are reported in. Jul 12, 2012 lothar rottmann from thermo scientific gives us a detailed tour of their new icap q icpms system that has been designed from the ground up. Powerful interference reduction for reliable and accurate quantification. Users can switch between single and triple quadrupole modes within a single multielement experiment.
Overview to scale the picture below is a simulation at scale of the thermo icap q icpms mass spectrometer system, installed on a ionbench ms mass spec benchtable. For information about the operating procedures for the. Placing the ms system thermo fisher scientific icap q preinstallation requirements guide pn 1288020, revision a 25. Novel qcell technology for inference removal in icpms. The installation of your icap q icp ms cannot be scheduled until this form is completed and returned to the above address. Unfortunately as from july we have been having problems with performance checks. These ions are then separated and detected by the mass spectrometer. Elemental scientific designs and produces a full range of automation and sample introduction systems for the determination of trace element concentrations in liquid samples by inductively coupled plasma instrumentation. The entry level icap qa icp ms provides multielemental analytical capabilities without the need to invest in collision cell technology. Inductively coupled plasmamass spectrometry icp ms is a powerful tool for analyzing trace metals in environmental samples.
There is a container on the work bench of the icpms lab room 204a designated for. Trace element speciation using ic icp ms analysis of lithiumion battery degradation products duration. Connect peripheral devices in minutes, thanks to an openaccess, sample introduction area. Icpoes has much higher tolerance for tds up to 30%. Faster method development for improved productivity. The coupling of the ics5000 ion chromatographic system with the icap q icpms has been shown to be a powerful tool for the detection of low concentrations of arsenic species in fruit juices. Inductively coupled plasma mass spectrometry icpms is a type of mass spectrometry that uses an inductively coupled plasma to ionize the sample. A large range of elements can be detected using an icpms, which are summarized in figure 1 below.
To demonstrate how simultaneous determination of all elements of interest in a wide range of food samples. Icap is an open protocol and allows any server or application provider to implement it. The ion source, icp is an ideal ionization source for mass spectrometry, and can ionize over 90% of many elements. Userinspired hardware and software combine in the thermo scientific icap rq icpms to deliver maximized productivity and robustness. Analysis of dissolved trace elements in aqueous solutions by icp.
Miscellaneous pictures pn description quantity 1600550 inline water filter 5. A new icicpms method for the separation and quanti. Routine 247 workhorse for laboratories upgrading from aa or the icap qc icp ms is configured for high icp oes. Pdf on apr 7, 2015, martin tanner and others published icptof by tofwerk, status march 2015 find, read and cite all the research you need on researchgate. Delivering triple quadrupole technology, the thermo scientific icap tqs icp ms is a highperformance icp ms for ultratrace quantification of trace elements in a variety of challenging matrices related to the semiconductor industry. If you try to attach a file format that is not accepted, you will see this message. In order to comply with the requirements described above for 21 cfr part 11 compliance, the thermo scienti.
To prevent viruses, malware and other malicious content from entering your organization, goanywhere mft can integrate with antivirus solutions using the standard icap protocol. Thermo fisher scientific introduces new icpms system, icap q. Although both icpoes and icpms can be used for high matrix samples, sample dilution is often necessary for use on icp ms. The interface is the region where ions generated in the plasma are transferred from atmospheric pressure to the vacuum region and introduced to the mass spectrometer as an ion beam. Without reaction finder with reaction finder select select the analytes to be measured select. Analysis of pharmaceutical products for their elemental impurities using the. This icap q operating manual contains precautionary statements that can prevent personal injury, instrument damage, and loss of data if properly followed. Workflow, data management, scalability and compliance.
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